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EFFICACY OF CONCRETE ROOF TILES COMPOSITE USING CLAY AND RICE STRAW

FIBRE AS HEAT INSULATION MATERIAL

AN NISHA NUR WELLIANA BINTI ABD RASED

UNIVERSITI SAINS MALAYSIA

2019

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EFFICACY OF CONCRETE ROOF TILES COMPOSITE USING CLAY AND RICE STRAW

FIBRE AS HEAT INSULATION MATERIAL

by

AN NISHA NUR WELLIANA BINTI ABD RASED

Thesis submitted in fulfillment of the requirements for the degree of

Doctor Philosophy

JANUARY 2019

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ACKNOWLEDGEMENT

I would like to express my very great appreciation to my supervisor Associate Professor Ts. Dr. Noor Faisal Bin Abas, for the patient guidance, encouragement and advice that he had provided throughout my time as his student. I have been extremely lucky to have a supervisor who cared so much about my work, and who responded to my questions and queries so promptly. I would also like to offer my special gratitude to my second supervisor Professor Ar. Dr. Abdul Malek Rahman for the advice given and had been a great help in my journey to complete my thesis.

My sincere gratitude to Mr. Islah Bin Mohamed Said, my husband, for his continuous support in giving advice, contributed additional funding and also endless encouragement. I am amazed by his willingness to proofread countless pages of my research. Not forgetting, the patience of my mother (Sa’diah Binti Awang), sister, brother and my daughter (Annur Khairina Binti Islah) who experienced all of the ups and downs of my research.

My special thanks are extended to the staffs of concrete and structure lab, metal and wood workshop, soil and land survey lab, school of Housing Building and Planning (HBP), Universiti Sains Malaysia because they had assisted and supervised me in the lab work. Completing this study would have been more difficult if not for the support and friendship provided by the other members of the School of HBP. I am indebted to them for their help.

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Last but not least, I would like to thank the Fundamental Research Grant Scheme (FRGS) and MyBrain15 programme for financing my postgraduate studies by Ministry of Higher Education (MOHE).

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TABLE OF CONTENTS

ACKNOWLEDGEMENT ……… ii

TABLE OF CONTENTS ……… iv

LIST OF TABLES ……….. x

LIST OF FIGURES ……… …… xii

LIST OF ABBREVIATIONS……… xvii

ABSTRAK ……….. xix

ABSTRACT ……… xxi

CHAPTER 1 - INTRODUCTION 1.1 Background of study……… 1

1.2 Present Scenario in Malaysia ……….. 12

1.3 Research Problem Statement ………..… 15

1.4 Research Questions……… 20

1.5 Research Aims and Objectives ……….. 21

1.6 Scope and Limitation of the Research……….... 22

1.7 Significant of Research ……….. 25

1.8 Outline of Thesis ………... 25

CHAPTER 2 - LITERATURE REVIEW 2.1 Introduction ……….. 29

2.2 Introduction of Concrete Roof Tile (CRT) ……….. 33

2.3 Constituent Materials of Concrete Roof Tile Composite (CRTC) …….. 35

2.3.1 Ordinary Portland cement ……… 36

2.3.2 Sand ………. 37

2.3.3 Clay ……… 38

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2.3.3(a) Sayong kaolinite clay ……….. 44

2.3.3(b) Advantages of clay ………... 45

2.3.3(c) Disadvantages of clay ……….. 47

2.3.4 Natural Fibre (Rice Straw) ……….... 51

2.3.4(a) Chemical constituents of natural fibre ………….. 52

2.3.4(b) Rice Straw Open-Field Burning ……..……… 54

2.3.4(c) Alternatives to Open-Field Burning……… 57

2.3.4(d) Advantages of rice straw ……… 58

inclusion in building material 2.3.4(d) Disadvantages of rice straw ………. 62

Inclusion in building material 2.4 Composite Material ……… 65

2.4.1 The Properties of the Fibre in composite material …………..…. 66

2.4.2 The Properties of the Resin ……… 68

2.4.3 The Amount of Fibre in the Composite ……….... 68

2.4.4 The Geometry and Orientation of the Fibre in the Composite ….. 69

2.4.5 The Surface Interaction of Fibre and Resin (The ‘Interface’) …... 70

2.5 Design Procedures and Methods of CRTC Production ……… 70

2.6 Workability ……… 71

2.7 Engineering Properties of Concrete Roof Tile Composite………... 72

2.7.1 Compressive Strength ……….. 73

2.7.2 Transverse Breaking Strength Test ………... 74

2.7.3 Water Absorption ………. 76

2.7.4 Water Permeability ……….. 77

2.7.5 Shrinkage ………. 77

2.8 Thermal Performance Test ……….. 78

2.8.1 Thermal conductivity ……….. 78

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2.8.2 Specific heat capacity ………..…. 81

2.8.3 Thermal diffusivity ………... 82

2.8.4 IR Thermography Test ………. 83

2.8.5 Actual house model indoor thermal performance ………... 84

2.8.6 Thermal simulation data ……… 85

CHAPTER 3 - RESEARCH METHODOLOGY AND CHARACTERISTIC OF MATERIAL 3.1 Introduction ……… 90

3.2 Experimental Programed Design ………... 91

3.2.1 Preparation and characterisation of materials………. 91

3.2.2 Concrete mix design……… 92

3.2.3 Physical and mechanical performance test……….. 93

3.2.4 Thermal conductivity and thermal imaging performance test.. 93

3.2.5 House model thermal performance test……..……… 94

3.3 Materials ………. 96

3.3.1 Cement ……… 97

3.3.2 Fine Aggregate ……… 99

3.3.3 Clay ………. 102

3.3.4 Water ………... 106

3.3.5 Rice Straw Fibre ……….... 106

3.4 Concrete Roof Tile (CRT) Design ………. 110

3.4.1 Mix Design and Proportions ………... 110

3.4.2 Mixing Procedures ……….. 114

3.4.3 Curing Regimes ……….. 116

3.5 Concrete Roof Tile Pefomance ……… 117

3.6 Workability (Flow Table test )………... 118

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3.7 Density of hardened concrete ………. 120

3.8 Mechanical properties of concrete ……… 121

3.8.1 Compressive strength test ………. 121

3.8.2 Transverse breaking strength test ………. 123

3.8.3 Impact Test ………... 125

3.8.4 Water absorption test ………... 125

3.8.5 Water permeability test ………. 126

3.8.6Shrinkage test ………... 127

3.9 Thermal Properties of concrete roof tiles composite …………... 129

3.9.1 Thermal conductivity test ……….. 130

3.9.2 Thermal imaging performance test………. 133

3.9.3 House model thermal performance test ……… 134

3.9.4 Simulate of concrete roof tile thermal ………. 140

performance 3.9.4(a) Thermal Condition templates …………. 140

3.9.4(b) Construction template manager ……….. 143

3.9.4(c) Setting the site and weather data……….. 146

3.9.4(d) Running Apachesim ……… 147

CHAPTER 4 - PROPERTIES OF CONCRETE ROOF TILES COMPOSITE 4.1 Introduction ………... 148

4.2 Workability of concrete ……… 149

4.3 Bulk Density of Concrete ………. 153

4.4 Compressive Strength ……… 161

4.5 Flexural Strength ……….. 170

4.6 Impact Strength ……… 178

4.7 Water Absorption ………. 181

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4.8 Drying Shrinkage ……….. 188

4.9 Water Permeability ………... 194

CHAPTER 5 - THERMAL PROPERTIES OF CONCRETE ROOF TILES COMPOSITE 5.1 Introduction……….. 196

5.2 Thermal Conductivity of CRT ………. 196

5.3 Specific heat capacity of CRT ……… 200

5.4 Thermal Diffusivity ………. 201

5.5 Thermal Resistance ……… 202

5.6 Thermal Tests Using Infrared Thermography ……… 203

5.7 Thermal properties of actual house model ……….. 205

5.8 Thermal test result from IESVE simulation for sample C10RS 1A …… 214

5.9 Comparison simulation data with actual result data ……… 226

5.10 Simulate the CO sample thermal data ………. 228

5.11 Summary of chapter 5……… 238

CHAPTER 6 - CONCLUSIONS AND RECOMMENDATIONS 6.1 Workability of CRTC ……….. 240

6.1.1 Flow Table test of CRTC ………. 240

6.1.2 Bulk density of CRTC ……….. 241

6.2 Engineering properties of CRTC ………. 242

6.2.1 Compressive strength of CRCT ……….. 243

6.2.2 Flexural strength of CRTC ……….. 243

6.2.3 Impact Strength of CRTC ………... 245

6.3 Durability of concrete roof tile composite (CRTC) ……… 246

6.3.1 Water Permeability Test ………. 246

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6.3.2 Water absorption of CRTC ………. 246

6.3.4 Drying shrinkage of CRTC ………. 248

6.4 Thermal performance of CRTC ……….. 248

6.4.1 Thermal conductivity CRT ………. 248

6.5 Thermal imaging of CRT ……… 250

6.6 Thermal properties of the house model ……….. 250

6.7 Comparison of actual data with simulation data for C10RS 1A ………. 251

sample 6.8 CO sample simulation data ………. 251

6.9 Main conclusion………. 252

6.10 Recommendation for future research ……….. 253

REFERENCES ……… 254 APPENDIX

LIST OF PUBLICATION

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LIST OF TABLES

Page Table 1.1 Percentage compositions of rice straw 8 Table 1.2 Mean data for meteorological and environmental data for each site 13

Table 2.1 Chemical compositions of untreated Sayong kaolinite clay 44

Table 2.2 Transverse breaking strength, min, Lbf (N) 75

Table 2.3 Water absorption range 76 Table 3.1 Chemical composition of standard OPC (Malaysia Standard 98 MS522: Part 1:2007) Table 3.2 Chemical composition of OPC used in present study 98 Table 3.3 Physical properties of cement 99 Table 3.4 Sieve analysis of fine aggregate (sand) by ASTM C 144-03 100

Table 3.5 Sieve analysis of fine aggregate (sand) used in the present 101

study Table 3.6 Properties of fine aggregate (sand) 102

Table 3.7 Chemical composition and physical properties of Sayong clay 104

Table 3.8 Chemical composition of rice straw fibre 108

Table 3.9 Result properties of rice straw 109

Table 3.10 Mix Design Proportions of 40concrte roof tile smaple 112

Table 3.11 Experimental of concrete properties 117

Table 4.1 Slump test result 149

Table 4.2 Density of all samples 153

Table 4.3 Compressive strength of all samples at the given curing age 161 and mixes proportions

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Table 4.4 Compressive Strength relative to the CO sample 164

Table 4.5 Flexural strength for all concrete samples 172

Table 4.6 Flexural strength relative to the CO sample 173

Table 4.7 Impact strength of concrete roof tiles 178

Table 4.8 Water absorption of all concrete samples 182

Table 4.9 Water absorption and density of CRT 182

Table 4.10 Drying shrinkage of all samples 189

Table 4.11 Water permeability of all concrete samples 194

Table 5.1 Average of thermal conductivity concrete roof tiles 197

Table 5.2 Thermal Resistance of concrete roof tiles 203

Table 5.3 Temperature result indoor and outdoor for 4 days (29, 30, 31 206

May 2017 and 1 June 2017) Table 5.4 Relative temperature between indoor and outdoor temperature 209

Table 5.5 IESVE temperature result (29 May 2017) – C10RS 1A sample 220

Table 5.6 IESVE temperature result (30 May 2017) – C10RS 1A sample 222

Table 5.7 IESVE temperature result (31 May 2017) – C10RS 1A sample 223

Table 5.8 IESVE temperature result (01 June 2017) – C10RS 1A sample 224

Table 5.9 The mean of comparison temperature by actual and simulate 225

data Table 5.10 The variance and standard deviation data 226

Table 5.11 IESVE temperature result (29 May 2017) – CO sample 231

Table 5.12 IESVE temperature result (30 May 2017) – CO sample 232

Table 5.13 IESVE temperature result (31 May 2017) – CO sample 233

Table 5.14 IESVE temperature result (01 June 2017) – CO sample 234

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LIST OF FIGURES

Page

Figure 1.1 Pore size arrangements in clay 5

Figure 1.2 Particle board 10

Figure 1.3 Medium density fibre board 11

Figure 1.4 Straw board 11

Figure 1.5 Cement bonded board 11 Figure 2.1 Tetrahedral sheet linked with oxygen 41

Figure 2.2 Octahedral sheet linked with oxygen 42

Figure 2.3 Kaolinite structure 43

Figure 2.4 Electron micrographs of Sayong kaolinite clay 43 Figure 2.5 Modulus of elasticity for crushed clay brick aggregate as a) 50 fine aggregate, b) coarse aggregate and c) coarse and fine aggregate Figure 2.6 Concrete sample with fibre imprints 64

Figure 2.7 Effect of straw content on heat energy released (ET) and 67

hydration rate (R) for untreated straw-cement composites Figure 2.8 Concrete roof tile setting for flexural strength 75 Figure 3.1 Flow chart of experimental programmed 95

Figure 3.2 Vibratory sieve machine 100

Figure 3.3 Particle size distributions of fine natural aggregates 101

Figure 3.4 Particle size analysis and density of Sayong clay 104

Figure 3.5 X-ray Diffraction pattern of Sayong clay 104

Figure 3.6 Crusher machine 105

Figure 3.7 Clay lumps and clay powder 105

Figure 3.8 Rice straw fibres 108

Figure 3.9 Instron testing machine (tensile strength test for rice straw) 108

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Figure 3.10 Cube mould 114

Figure 3.11 Prism mould 114

Figure 3.12 Plate mould 115

Figure 3.13 Flow Table test setup 118

Figure 3.14 ELE compression testing machine 120

Figure 3.15 Satisfactory failures of concrete cubes 120

Figure 3.16 Unsatisfactory failures of cubes concrete 121

Figure 3.17 Traverse breaking strength test 123

Figure 3.18 Impact test setup 123

Figure 3.19 Water absorption test apparatus 125

Figure 3.20 Water Permeability Test 126

Figure 3.21 Length comparator 128

Figure 3.22 Mould of cylinder concrete 130

Figure 3.23 Hot Disk Thermal Constants Analyser Apparatus 131

Figure 3.24 Hot Disk Thermal Constant Analyser with test samples 131

Figure 3.25 Schematic of Samples and Sensor for the Hot Disk 131

Figure 3.26 Hot Disk sample holder with cover 132

Figure 3.27 Infrared thermal imaging cameras 133

Figure 3.28 Samples of concrete roof tile composite 134

Figure 3.29 Casting of concrete roof tile composite 134

Figure 3.30 Actual house model in graphical 135

Figure 3.31 Actual house model image 136

Figure 3.32 Setting of thermocouple apparatus 137

Figure 3.33 Apparatus setup in building plan 137

Figure 3.34 Apparatus setup in isometric view 138

Figure 3.35 House model drawing 140

Figure 3.36 Weekly profiles database System 141

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Figure 3.37 Room condition tab image 141

Figure 3.38 Internal gains setup 142

Figure 3.39 Save the thermal condition setup 142

Figure 3.40 Construction template manager setup 143

Figure 3.41 Button to get the construction database 143

Figure 3.42 The system constructions window 144

Figure 3.43 Add the other unsuitable concrete data 145

Figure 3.44 Close the construction data 145

Figure 3.45 Aplocate utility systems 145

Figure 3.46 Button of Apachesim (dynamic simulation) 146

Figure 3.47 Save button 146

Figure 3.48 Simulate button 146

Figure 4.1 Flow diameter of fresh normal concrete, concrete with 10% 150

clay, concrete with 1% rice straw and concrete with 10% clay and 1% rice straw (0.1cm – 2.0cm Figure 4.2 Slump of fresh concrete mix with inclusion various percentage 151

of clay Figure 4.3 Slump of fresh concrete with various rice straw fibre volume 152

fractions Figure 4.4 Densities of normal concrete, concrete with 10% clay, 155

concrete with 1% rice straw and concrete with 10% clay and 1% rice straw (0.1cm – 2.0cm) Figure 4.5 Densities of concrete samples with various percentage of clay 155

Figure 4.6 Densities of concrete with various volume fractions of rice straw 157 fibre Figure 4.7 Densities of concrete with various lengths of rice straw fibre 158 Figure 4.8 Densities of concrete with 10% clay and various volume fraction 159

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xv of rice straw fibre (0.1-2.0cm)

Figure 4.9 Densities of concrete with 10% clay, 1% rice straw and various 160 lengths of rice straw fibre

Figure 4.10 ensities of concrete with various ratios of clay percentage, 1% 161 rice straw (0.1-2.0cm)

Figure 4.11 The compressive strength of normal concrete, concrete with 166 10% clay, concrete with 1% rice straw and concrete with

10% clay and 1% rice straw (0.1cm – 2.0cm)

Figure 4.12 Compressive strength of concrete sample with various 167 clay percentages

Figure 4.13 Compressive strength of hybrid form concrete with various clay 168 percentage

Figure 4.14 Compressive strength of concrete with 10% clay percentage 169 and various rice straw fibre percentage (0.1-2.0cm)

Figure 4.15 Compressive strength of concrete with 10% clay percentage, 170 1% rice straw volume fraction and different rice straw fibre

lengths

Figure 4.16 Flexural strength of normal concrete, concrete with 10% 174 clay, concrete with 1% rice straw and concrete with 10% clay

and 1% rice straw (0.1cm – 2.0cm)

Figure 4.17 Flexural Strength of tested samples with various percentage 175 of clay

Figure 4.18 Flexural Strength concrete with various volume fractions of rice 175 straw fibre

Figure 4.19 Flexural strength of tested samples with 10% clay percentage, 176 1% rice straw and various length of rice straw

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Figure 4.20 Flexural strength of concrete with various percentages of clay, 177

1% rice straw (0.1-2.0cm) Figure 4.21 Water absorption of normal concrete, concrete with 10% clay, 183

concrete with 1% rice straw and concrete with 10% clay and 1% rice straw (0.1cm – 2.0cm) at 28 days curing age Figure 4.22 ater absorption of normal concrete, concrete with 10% clay, 184

concrete with 1% rice straw and concrete with 10% clay and 1% rice straw (0.1cm – 2.0cm) Figure 4.23 Water absorption graph of samples in the various clay 186

percentages Figure 4.24 Water absorption of concrete sample in various volume 187

fractions and various lengths of rice straw fibre Figure 4.25 Water absorption of concrete with various clay percentage, 1% 188

rice straw (0.1-2.0cm) Figure 4.26 Drying shrinkage of normal concrete, concrete with 10% clay, 190

concrete with 1% rice straw and concrete with 10% clay and 1% rice straw (0.1cm – 2.0cm) Figure 4.27 Drying shrinkage of clay concrete at various percentage of clay 191

Figure 4.28 Drying shrinkage of rice straw concrete at various percentage of 192

rice straw volume fractions Figure 4.29 Drying shrinkage of clay concrete with10% clay percentage, 1% 193 rice straw and various rice straw fibre lengths Figure 5.1 The average thermal conductivity of concrete roof tiles samples 197

Figure 5.2 Thermography images of CO sample and CRS sample 204

Figure 5.3 Actual house model 205

Figure 5.4 Apparatus setup inside and outside the building 206

Figure 5.5 Temperature graph on 29 May 2017 211

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Figure 5.6 Temperature graph on 30 May 2017 211

Figure 5.7 Temperature graph on 31 May 2017 212

Figure 5.8 Temperature graph on 1 June 2017 212

Figure 5.9 Temperature graph at 31 May (4:00 PM until 8:00 AM) 213

Figure 5.10 Assigned thermal of roof (C10RS 1A) 214

Figure 5.11 Assigned thermal of ceiling (C10RS 1A) 215

Figure 5.12 Assigned thermal of door (C10RS 1A) 215

Figure 5.13 Assigned thermal of floor (C10RS 1A) 216

Figure 5.14 Assigned thermal of internal partition (C10RS 1A) 216

Figure 5.15 Assigned thermal external walls (C10RS 1A) 217

Figure 5.16 Assigned thermal of windows (C10RS 1A) 217

Figure 5.17 C10RS 1A thermal properties result of HBP model house using 218

Apache setting in IESVE software. Figure 5.18 Roof visual image of HBP model house using IESVE software 218

Figure 5.19 Sunrise direction using Sun cast setting in IESVE software 219

Figure 5.20 Model House Temperature at 29 May 2017 (C10RS 1A sample) 227

Figure 5.21 Model House Temperature at 30 May 2017 (C10RS 1A sample) 227

Figure 5.22 Model House Temperature at 31 May 2017 (C10RS 1A sample) 228

Figure 5.23 Model House Temperature at 01 June 2017 (C10RS 1A sample) 228

Figure 5.24 Assigned thermal of roof (CO sample) 229

Figure 5.25 C10RS 1A thermal properties result of HBP house model using 300

Apache setting in IESVE software. Figure 5.26 House model temperature at 29 May 2017 (CO sample) 236

Figure 5.27 House model temperature at 30 May 2017 (CO sample) 237

Figure 5.28 House model temperature at 31 May 2017 (CO sample) 237

Figure 5.29 House model temperature at 01 June 2017 (CO sample) 238

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LIST OF ABBREVIATIONS

CO Control concrete

CPC Climate Prediction Centre CRS Concrete Rice Straw CRT Concrete Roof Tile

CRTC Concrete Roof Tile Composite GJ Gigajoule

GPa Giga Pascal

IESVE Integrated Environmental Solutions (Virtual Environment) LEED Leadership in Energy Environmental Design

MPa Mega Pascal NaOH Sodium hydroxide ONI Oceanic Nino Index PP Polypropylene RS Rice straw SiO2 Silicon dioxide SiO44- Orthosilicate [Si4O10]4- Tetrahedral XRD X-ray Diffraction XRF X-ray Fluorescence HTV Hybrid Turbine Ventilator

HVAC Heating, ventilation, and air conditioning

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KECEKAPAN JUBIN BUMBUNG KONKRIT KOMPOSIT MENGGUNAKAN TANAH LIAT DAN GENTIAN JERAMI PADI

SEBAGAI BAHAN PENEBAT HABA

ABSTRAK

Pada masa ini, jubin bumbung konkrit komposit (CRTC) dengan pelbagai peningkatan sifat sering digunakan sebagai penutup bumbung. Hal ini disebabkan oleh kelebihannya yang tahan sangat lama dan bertahan selama bertahun-tahun, dapat menahan angin kencang yang lebih baik daripada bahan lain, kos yang terlibat lebih rendah, lebih mudah diperolehi dan juga pengeluaran yang tinggi karana sangat mudah untuk dihasilkan. Penyelidikan ini tertumpu kepada sifat kejuruteraan, ketahanan dan sifat terma CRTC yang dihasilkan daripada pelbagai nisbah tanah liat dan serat jerami padi. Impak terhadap perbezaan panjang serat jerami padi juga telah diuji dalam kajian ini. Ciri-ciri jubin bumbung konkrit (CRT) juga telah diuji mengikut ASTM C1492 - 03 (2016) Spesifikasi piawaian jubin bumbung Konkrit dan kebolehmampuan CRT ini diuji dengan berdasarkan Kaedah Ujian Piawaian Aliran Mortar Hidraulik Simen (ASTM C1437). Prestasi terma seperti kekonduksian terma, kapasiti haba tertentu dan kelesapan haba telah diukur menggunakan Model Analisa Pemalar Haba Cakera Panas TPS 2500. Manakala, terma inframerah (imej IR) digunakan bagi mendedahkan perilaku terma yang berlaku keatas C10RS 1A berbanding sampel konkrit kawalan (CO). Prestasi terma dalaman diukur dengan menggunakan model rumah sebenar dan kaedah simulasi IESVE. Selepas itu, data dari kedua-dua kaedah ini dibandingkan dan digunakan untuk mendapatkan data sampel CO melalui simulasi IESVE. Hasil daripada keseluruhan ujian,

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sampel C10RS 1A yang mempunyai campuran tanah liat dan gentian jerami padi mempunyai sifat kejuruteraan yang rendah tetapi ia bahan yang ringan, tahan hentakan dan kebolehtelapan air tinggi. Ia juga mempunyai kekonduksian terma yang rendah, kapasiti haba tertentu yang tinggi dan pembesaran haba yang rendah daripada sampel konkrit kawalan (CO), konkrit dengan campuran 10%

tanah liat (C10) dan konkrit dengan campuran 1% jerami padi - 0.1cm -2.0cm (RS 1A). Purata ΔT C10 di dalam bangunan pada suhu maksimum adalah lebih rendah daripada suhu luar iaitu 3.68 ºC (semasa waktu paling panas) dan 0.65 ºC (semasa waktu paling redup). Jika dibandingkan dengan C10RS 1A, yang mempunyai purata ΔT iaitu 4.73 °C (semasa waktu paling panas) dan 1.70 °C (semasa waktu paling redup). Hasil ini menunjukkan konkrit dengan tanah liat dan serat jerami padi mempunyai kadar pemindahan haba yang lebih rendah dan menyerap haba matahari yang kurang daripada konkrit dengan tanah liat.

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EFFICACY OF CONCRETE ROOF TILE COMPOSITE USING CLAY AND RICE STRAW FIBRE AS HEAT INSULATION MATERIAL

ABSTRACT

Currently, concrete roof tile composite (CRTC) with various properties improvement is frequently used for roof covering. This is mainly due to the advantages such as they are very durable and last for many years, can withstand high winds better than other materials, lower costs involved, more readily available and also production is high because it is easily manufactured. This research mainly focuses on the engineering, durability, and thermal properties of concrete roof tile (CRT) that were produced with various ratios of clay and rice straw fibre. The impacts of different lengths of rice straw fibre were also tested in this study. The CRT properties were tested followed ASTM C1492 - 03(2016) Standard Specification for Concrete Roof Tile and the workability of this CRT was tested according to Standard Test Method for Flow of Hydraulic Cement Mortar (ASTM C1437). Thermal performance like thermal conductivity, specific heat capacity and thermal diffusivity was measured using Hot Disk Thermal Constants Analyser Model TPS 2500. Besides that, the infrared thermography (IR image) was used to reveal the expected thermal behaviour of concrete with 10% clay and 1% rice straw (0.1 cm-2.0cm) C10RS 1A compared to control concrete (CO) sample. Indoor thermal performance was measured by using actual house model and IESVE simulation method. After that, the data from these two methods were compared and utilized in order to obtain the CO sample data via IESVE simulation. Results from the entire test proved that C10RS 1A sample with clay and rice straw has low engineering properties but it is lightweight, high shock resistant and high water resistance. It also

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has lower thermal conductivity, higher specific heat capacity and lower thermal diffusivity than CO, concrete with 10% clay (C10) and concrete with 10% rice straw - 0.1cm – 2.0cm (RS 1A) samples. The mean of ∆T of C10 inside the building at maximum temperature was lower than outside temperatures which were 3.68 ºC (during hottest hours) and 0.65 ºC (during cloudiest t hours). Comparing to C10RS 1A, that has the mean of ∆T which were 4.73 °C (during hottest hours) and 1.70 °C (during cloudiest hours). This result shows concrete with clay and rice straw fibres has lower heat transfer rates and absorb less solar heat than concrete with clay.

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1 CHAPTER 1

INTRODUCTION

1.1 Background of Study

Concrete is the most generally used construction material in the world as a result of its versatile properties and economical price compared with the other materials.

Concrete roof tile has long been in use as a roof covering for providing a stable and reliable engineering material. It provides certain benefits, remarkably solid product, can stand up to wind and storms, longer durability and more cost-effective than alternative building material that it competes with an excellent combination of its durability. Yet, the concrete roof tiles are fairly heavy and also the production is unconcerned about the amount of thermal efficiency. However, the usage of standard concrete roof tile has some limitations depending on the weather within the specific country.

Green certification programs like LEED, Energy Star, the U.S. Green Building Council and the Department of Energy Building Technology Program base their respective cool-roof credentials should have properties like an ability to reflect the sun (solar reflectance) and unleash absorbed heat (emissivity). The higher solar reflection factor and emissivity (on a scale from 0 to 1), the roof will be cooler.

Asian countries receive a large quantity of solar radiation, heat, high level of relative humidity, and long periods of sunny days throughout the year. Besides than

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that, the increased urbanization create development is simply too quick and densely at city space. It causes the rising temperatures and accrued the intensity of urban heat island (UHI) (Wong and Yu, 2011).

Insulation may be a key part of property building style. A properly insulated home reduces energy bills by maintaining cool throughout the hot time and turn lowers carbon emission affecting international temperature change. Referring to energy efficiency, committing to high amounts of insulation materials for residence is cheaper than buying expensive cooling technologies. It is really worth making the effort to search out the proper materials instead of changing the whole building design.

Insulation materials are widely used in roofs, walls and floors. Natural insulation products have various benefits over typical materials. They are low impact, made up of renewable, organic resources and have fully low embodied energy. They will be reused and recycled, and therefore are fully biodegradable.

They are non-toxic, allergen-free that permits it to be safely handled and installed.

Therefore, a lot of analysis within the development of a new roof design and materials has been carried out. Engineers and scientists within the construction industry have proposed the use of cool roof, an upgraded and enhanced version of existing roof material. Much progress has been made within the development of roof style and material like using modified bitumen, single ply membrane, add a coat of cool, use a metal material, use an evaporative cooling system and different ways to create a cool roof.

Unfortunately, natural insulation materials are nearly 4 times pricier than standard materials, which might be a burden to builders, architects, and developers

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(Gray, 2018). Apart from that, there are many problems that require confronted in dealing such as no long life cycle, need skilled labour, used high technology, and takes an extended time to provide additionally high maintenance cost. Even so, the environmental and health advantages of natural insulation materials decrease their prices, and growing consumer demand beside government regulation and rising oil costs can inevitably drive costs down. Natural insulation is usually an energy- efficient, healthy and sustainable choice for a better outdoor and indoor environment.

As the solution of this issue, the sustainable world’s economic growth and people’s life improvement greatly depend upon the utilization of different product within the design and construction, like sources of soil-based materials wastes natural material. They will be obtained at low price and low levels energy using local manpower and technology (Frybort et al., 2008). Concrete roof tile composites manufactured from cement, clay and lignocelluloses materials have several benefits such as higher strength, higher resistance to bio deterioration and light-weight, able to function as a thermal barrier, does not has formaldehyde emission originating from the binder and might be used as means of recycling wood residues.

On the other hand, the manufacture of ordinary Portland cement (OPC) could be extremely energy intensive and environmentally unfriendly method needed regarding 4GJ (gigajoule) of energy per ton of the finished product (Bahnsawy et al., 2015). Furthermore, the contribution of Portland cement production worldwide to the gas emission is calculable to be regarding 1.35 billion ton annually or about 7% of the entire gas emission to the earth atmosphere (Malhotra, 2002). Most cement kilns these days use coal and petroleum coke as primary fuels and, to a lesser extent, natural gas and fuel oil.

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Cement manufacture causes environmental impacts at all stages of the process. These include emissions of airborne pollution within the variety of dust, gases, noise and vibration once in operation machinery and through blasting in quarries and damage to countryside from quarrying. Directly through the production of CO2 (carbon dioxide) once calcium carbonate is heated, manufacturing lime and CO2 and indirectly through the employment of energy, particularly the energy is sourced from fossil fuels. The cement industry produces regarding 5% of total global CO2 emissions, of that 50% is from the chemical process, and 40% from burning fuel. The quantity of CO2 emitted by the cement trade is almost 900kg of CO2 for each ton of cement production (Bakhtyar, 2017).

In order to produce environmentally friendly concrete, Mehta (2002) suggested the utilization of fewer natural resources, less energy, and minimize CO2

emissions. McCaffrey (2002) suggested that the amount of CO2 emissions by cement industries will be reduced by decreasing the number of calcined material in cement, by decreasing the number of cement in concrete, and by decreasing the amount of buildings using cement.

Currently, the cement which will be used for building purpose is extremely costly and has gone beyond the reach of the low-income earners. These demand different sources of building materials. Examination of some different sources of soil-based materials establishes that there are several soil resources that are appropriate for construction. One among this soil-based is clay, wherever it is used as a cement replacement, will improve indoor temperature and also can reduce carbon emission. The previous study reveals, using clay brick will reduce the indoor temperature in 3% than mortar brick (Laaroussi et al., 2013). Besides, this fact also

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supported by Azhary et al. (2017), consequently the unfired clay bricks is a good insulating material because the decrease in the indoor temperature by an approximately 5.1°C during the hottest period in their study. Thomson et al. (2015) and they assert the most part to the exposed thermal mass that facilitate buffer the temperature and relative humidity of the indoor environment. There is also has a good material inclusion like mineral and organic aggregates to assist improve these thermal properties.

Clay is one of the oldest, contains a layer silicate mineral (called phyllosilicate) or different mineral that imparts plasticity and hardens upon drying or firing (Guggenheim and Martin, 1995). It might be referred to as a particle size in a soil or sediment of a diameter < 0.002 mm or 2 microns. Clay created from silica (SiO2), alumina (Al2O3) and water (H2O) plus significant concentrations of oxides of iron, alkali and alkaline earth. Figure 1.1 shows the pore size arrangement in clay.

Figure 1.1 Pore size arrangements in clay (Manic Botanix. Com, 2016)

Chemical properties of clay show the clay contains high amounts of silica and alumina but included crystalline structure. Therefore, it doesn't possess amorphous

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pozzolanic activity and the strength is lower than fired clay. Nevertheless, by heating treatment, including calcining between 700 ⁰C to 900 ⁰C, this crystalline structure is ruined and quasi-amorphous structure is acquired. Clay contains physical and mechanical properties as example plasticity, shrinkage under heating and under air-drying, fineness of grain, colour once firing, solidity, lightweight, cohesion, and capacity of the surface to take decoration. Clay is the healthiest and additionally the foremost effective substance that one can use in order to construct sustainable building material in development. Clay is "good thermal mass", it is superb in retaining temperatures at steady level. Clay holds heat or cold, releasing it over a period of your time such as stone. Clay may be a living, breathing building material which in fact enhances the air around it, absorbing and releasing humidity comparatively fast. This leads to naturally controlled level of wetness and with it a healthier space environment is attained. Hence, designing and building with clay can contribute considerably to cut energy used.

Lignocelluloses agricultural by products are obtainable on a worldwide basis and regarded from renewable resources. Lignocelluloses actually are massive and cheap source for cellulose fibres. Agro-based bio-fibres possess the composition, properties, and structure that create them ideal for multiple uses namely composite, textile, pulp, and paper production. Moreover, bio-fibres also can be used to produce fuel, chemicals, enzymes, and food. According to Bouasker et al. (2014), no doubt, natural fibres, such as hemp, flax, cotton, jute, sisal, pineapple, cereal straw can be used in a variety of manners. Other researcher Patel et al. (2013) assert that groundnut husk, jute fibre, rice husk, rice straw, rice bale, saw dust, and coconut

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fibre and other fibrous material have been identified as most economically important wastes for building industry.

Rice straw is one of the extremely considerable agricultural trashes and one of the natural fibres. The National Food Security aims to increase the National Self Sufficiency Level (SSL) of domestic rice production from 70% to 85% by 2015.

Malaysia needs to produce around 2.5 million metric tons of paddy annually (Rashid and Shah, 2013). That means, around the same volume of rice straw was produced in 2013. On the other hand, the rise in productivity and size of paddy areas, among different things, has resulted in enormous surplus of rice straw where the most cost- effective manner of getting rid of the residue is seen as burning the biomass within the paddy field that causes severe air pollution.

Rice straw contains a large quantity of fibre and features a nice potential to replace wood for the production of wide variety of composites. Producing composite materials from rice straw is probably going to contribute favourably to the disposal problem as well as to the overall CO2 balance as a carbon sink. Converting rice straw into added products has conjointly the potential to boost the performance of agriculture sector. The better utilization of rice straw will also benefit farmers as an extra financial gain, which can be a crucial motivating factor in promoting an efficient harvesting, collection and management of rice straw. Additionally, the industry is additionally showing increased interest in the production of composite materials from agricultural residues due to the accuse shortage of forest resources.

Rice straw is classified as non-wood fibres; it is most useful as fibre for construction supplies, papers and also as animal feeds. Among the various agricultural straws, rice straw could be very interesting material as filler in

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biodegradable polymer composites, due to its good thermal stability, competitive specific mechanical properties, and availability, low cost and lightweight compared to different agricultural waste (Buzarovska et al., 2008). According the study by Mansour et al. (2007) found that the cement straw slabs can be used in new construction as well as in existing buildings to improve the thermal insulation and acoustic absorption. The rice straw can effortlessly be grinded into chips or particles, which are terribly the same wood particles or fibres. It is also are obtainable on a global basis and thought of renewable materials. Rice straw will be obtained at low cost and low levels energy using local manpower and technology (Frybort, et al., 2008).

The rice straw is primarily contained in carbohydrate components like hemicelluloses, cellulose, and lignin Hamid and Zain, (2014). Table 1.1 shows the percentage composition of rice straw. A study by Sjostrom (1993) showed that the chemical constituents of natural fibre like rice straw have specialised functions within the cell wall: cellulose forms strong and stiff crystalline regions, cellulose and hemicelluloses form semi-crystalline regions provide necessary flexibility whereas the amorphous regions of lignin give toughness and cohesion.

Table 1.1 Percentage compositions of rice straw (Chandel et al., 2009)

Components Composition (%)

Cellulose 37

Hemicellulose 24

Lignin 14

Others 25

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The mechanical properties of natural fibres rely on its cellulose type because each type of cellulose has unique cell geometry which determines the chemical compositions. Hemicelluloses chains to cellulose by hydrogen bonding and acts as cross-linking molecules between the cellulose microbial forming the cellulose- hemicellulose network, which could be considered to be the primary structural part of the fibre cell. Lignin is the compound that provides hardness to the fibres. Rice straw fibres could not reach great heights or rigidity without lignin. The rice straw resistance to microbial decomposition and enables this material appropriate as filler in building composite materials. As an alternative, high content of silica (up to 20%) signifies a further potential benefit relating to the flame retardant once utilised in building industry. From this perspective, rice straw has been examined as possible filler in numerous thermoplastic matrices. According Yang et al. (2004) have analysed polypropylene filled with rice straw composites. They documented that it did elevate mechanical properties, i.e. increased tensile modulus of the PP/rice straw composites with the increase of filler content.

The rice straw skin features a waxy structure which can result in poor cohesiveness with cement. It offers tensile strength, as rebar does in concrete. Rice straw is unique relative to additional cereal straws in being low in lignin and high in silica. Rice straw fibres strength of 3.5 grams/denier (450 MPa), elongation of 2.2%, and modulus of 200 grams/denier (26 GPa), similar to linen fibres (Reddy and Yang, 2006). The untreated rice straw has the best tensile strength than treated by water and NaOH (Morsy et al., 2011). NaOH treatment decreases the strength than water treatment attributable to the elimination of amorphous compounds like lignin and hemicellulose. Concrete filler rice straw clearly reduce the maximum hydration

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temperature attained (T) and increase the time of achieves the maximum temperature (t) as compared with standard concrete (Morsy et al., 2011). Within the same study, rice straw cementitious composite has a potential to be used in the production of a new lighter building material like brick due to its low density than other fibre. Water absorption and thickness swelling of straw cementitious composites were in the same range of wood cement composite material.

The use of rice straw is to produce composite concrete roof tiles that will improve thermal performance, enhances mechanical performance and physical properties like high strength, high durability, low density and less absorb water vapour. According Patel et al. (2013), a lot of building material products that have been produced from rice straw (see Figures 1.2, 1.3, 1.4 and 1.5) and it is very useful and sustainable building material.

Figure 1.2 Particle board (Yang et al., 2003)

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Figure 1.3 Medium density fibre board (Alison Peng, 2016)

Figure 1.4 Straw board (Sokhansanj et al., 2004)

Figure 1.5 Cement bonded board (Mansour et al., 2007)

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This particle board uses as a sound absorbing and for inner walls and improves the mechanical strength and water absorption of medium density fibre board uses as a wall celling and furniture. It also improves mechanical strength, water resistance, and cutting tools wear. Straw board uses as a wall and roofing and also improves the mechanical strength. All of these material function as improved thermal and sound absorbing, mechanical strength, water absorption, water resistance and durability.

1.2 Present Scenario in Malaysia

Considering that Malaysia is within the tropical region and consists of thirteen states and three Federal Territories. The country of Malaysia is in the Asia continent and the latitude and longitude for the country are 4.1936ºN, 103.7249ºE. Kuala Lumpur is the capital city, although the administrative seat of government moved in 1999 to the newly designed Federal Territory of Putrajaya.

Recently, Malaysia has more established increased urbanization as results of the fast growth of the urban population. The highest populated states in West (Peninsula) Malaysia based on population density are Kuala Lumpur, Pulau Pinang, and Putrajaya. In East (Borneo) Malaysia, the Federal Territory of Labuan has a substantially denser population than the much larger states of Sarawak (capital town Kuching) or Sabah (capital town Kota Kinabalu). The local is equatorial characterised by annual southeast (April to October) and northeast (October to February) monsoons. It is obvious that we are dealing with great deal of issues with regards to the sun and the wind. It is an unpleasant climate zone that receives a huge

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amount of solar radiation, high temperature, high level of relative humidity, and extended periods of sunny days throughout the year. Reported by Meteorological Stations, Petaling Jaya, Malaysia has maximum temperatures 34°C on 29 January 2015. For that reason, it is actually a lot of crucial to avoid solar radiation coming back from warming the building surfaces.

Table 1.2 Mean data for meteorological and environmental data for each site (Engel- Cox et al., 2012).

Site Mean Daily

Dry Bulb Temp. (°C)

Relative Humidity

(%)

Average Wind Speed

(m/s)

Global Solar Radiation (kWh(m2d)

Subang (Kuala Lupur) 27.7 78.6 1.62 4.86

Kuantan 26.9 84.3 1.72 4.57

Sandakan 27.5 82.7 N/A N/A

Kota Baharu 27.3 81.4 2.19 5.11

Bayan Lepas (Penang) 27.8 79.4 1.84 5.1

Sitiawan 27.2 83.8 1.03 4.62

Melaka 27.5 80.6 1.55 4.5

Senai (Johor Bahru) N/A N/A 1.31 3.73

Labuan 27.9 80.7 N/A N/A

Kota Kinabalu 27.4 81 N/A N/A

Bintulu 26.9 83.3 N/A N/A

Miri 27.1 83.9 N/A N/A

Sibu 26.6 84.3 N/A N/A

Tawau 26.7 83 N/A N/A

Kuching 26.4 85.1 1.32 4.19

As shown in Table 1.2, Labuan (27.9°C) and Bayan Lepas (27.8°C) had high Yearly Temperatures whereas Kuching (26.4°C) had the lowest (Engel-Cox Nair, and Ford, 2012). Bayan Lepas (5.10 kWh/(m2d)) and Kota Baharu (5.11 kWh/(m2d)),

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both in the northern part of Peninsular Malaysia, have the highest mean daily global solar radiation.

As a results of the phenomenon is high temperature, higher relative humidity, substantial periods of sunny days throughout the year and huge of solar radiation, resulting in the rising temperature and even more increased the intensity of urban heat island (UHI). UHI phenomenon has shown that the materials utilized in urban development possess higher absorptive heat capacities than the soil and vegetative land cover that they replace (Bingfeng and Pingjun, 2007; Santamouris et al., 2011; Taha, 1997). The "hard" land surfaces such as roads, bridges, parking lots, walkways, patios, roofs, and walls have a tendency to absorb solar radiation incident on them and radiate the energy at night; raising the surrounding temperature (Synnefa et al., 2006). However the intensity and magnitude of the urban heat island vary from city to another, it might be simply defined by the distinction in temperature measured between urban and rural areas, (Streutker, 2003). The urban heat island has been delineated as a pillow of heat air on top of the city (Sham, 1987). The foremost typical and recorded index of the urban heat island is the increase of air temperature (Valazquez-Lozada, 2002).

The reason of Malaysia is in tropical climatic locations, passive cooling is among the foremost difficult issues to overcome. The economical and the only choice for effective cooling are by introducing air conditioning. Having said that, such equipment involves has high initial and operational costs for installation, electricity and routine maintenance. Consequently, air conditioners are unexpected to be used extensively in building, particularly for low-income earners. Nevertheless,

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additional way which can be used to reduce indoor temperature is use of sustainable building material.

Cautious analysis of thermal properties of materials is made use of within the development of urban areas is used as a way to alleviate UHI. This will readjust outdoor heat environment transfer to the indoors. The principal properties governing the thermal performance of materials include reflectance and emittance (Wong and Yu, 2012). Additionally, thermal conductivity is likewise a part of important properties that need to be explored. Another study by (Santamouris et al., 2011) revealed that the material with high reflectance and emittance tend to lower surface temperatures thus transfer less heat to their surrounding though convection. This situation occurs due to exposure of direct sun light; the roof has a huge impact on the thermal performance of the whole building (Badrul Hisham et al., 2005). Suehrcke, et al. (2008) reported that about 1kw/m2 of solar radiation falling on a roof surface during clear sky condition and from 20% to 95% of this solar radiation is absorbed.

The roof surface absorbs and reflects solar radiation as well as it has effects on surface temperature and indoor temperature of the building.

1.3 Research Problem Statement

Due to its location, Malaysia receives the sun directly overhead almost all of the days through the year. According director general from the Meteorological Department, Datuk Che Gayah Ismail said in New Straits Times on 24 February 2015, that the weather from the end of March until mid-May is the monsoon season. She also said the current temperature is between 33 and 35 degrees Celsius. This season causes

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many areas to receive less rain over an extended period, leading to the hot and dry weather. The temperature turned out to be more terrible when the drastically increment of population at dense area like Kuala Lumpur, the national capital and most crowded city in Malaysia.

According to CIA World Factbook, 2014 Percentage urban population in Malaysia is 72.8% of total population in Malaysia in 2011. It really makes increased urbanization due to the rapid growth of the urban population. Increasing of housing demand will definitely have an impact on the cost of construction or development and thus the selling price of residential houses. These circumstances occurred because increasing of building material demand and create the source of material become scarcer.

Due to the increasing of development, it is can cause the rising temperatures within the urban area and urban heat islands. Kuala Lumpur is among urban heat island in Malaysia and is usually several degrees hotter compared towards the surrounding countryside on heat summer days, the air in a city is usually 6-8°F hotter than its surrounding areas. The impact from this situation, the solar heat is reflected and absorbed into the building at once reduce indoor thermal comfort.

The solar heat received into the building by conduction through various building components like the wall, roof, ceiling, floor, etc. Heat transfer also takes place from different surfaces by convection and radiation. Besides, solar radiation is transmitted through clear windows and is absorbed by the interior surfaces of the building. This situation can make decrease the thermal performance of a building.

The thermal performance of a building depends on various factors namely design variables (geometrical dimensions of building components as an example walls, roof

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and windows, orientation, shading devices), material properties (density, specific heat, thermal conductivity, transmissivity), weather data (solar radiation, ambient temperature, wind speed, humidity); and also a building’s usage data (internal gains due to occupants, lighting and equipment, air exchanges).

As a result of this, major heat gain of Malaysian houses derives from the roof.

One of several major issues of Malaysian residential development would be the overheating of roof areas as results of inappropriate selection of roofing systems and materials. The unsuitable roofs which are used in the majority of new buildings do not resist the flow of heat in the hot day. This will cause the increase of the temperature during midday and also high indoor temperature compared to outdoor temperature at night.

Previous studies have shown that in Malaysian houses, the roof has a huge impact on the thermal performance of the whole building (Badrul Hisham, Samirah, Azni Zain, 2006; Nor Zaini, 2005). Once the heat gets into the rooftop space, the hot air heats up the inner structures and surfaces, and therefore the heat can likely be retained for most of the night. The excessive heat gained from the sun is radiated from the roof space to the occupants within the house through long wave radiation (Koenigsberger et al., 1980). According to previous studies, around 87% of heat transfer from the roof to occupant is through radiation process, whereby only around 13% of heat is transferred through conduction and convection (Cowan, 1973).

The above situation resulting in to the high cost of housing development, Malaysia has adopted several low-cost housing strategies, in an effort to compensate for growing housing demands. At present, the vast majority of housing units are used low cost and quality as a roof material, which is an adapted material from different

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climatic zones and countries with different types of natural resources. The use all of those substances as a building material can have a negative impact on the environment and people.

To overcome this problem the natural reinforcing materials can be obtained at low cost and low levels of energy using local manpower and technology and also low cost. Utilisation of natural fibres as a form of concrete enhancement is of particular interest to less developed regions where conventional construction materials are not readily available or are too expensive. Coconut and sisal-fibre reinforced concrete have been used for making roof tiles, corrugated sheets, pipes, silos and tanks (Agopyan, 1988).

Additionally, there are weaknesses in using the incorrect types of roof material like requires the high-density material, the high heat absorbent, fragile, easily mouldy, not long lasting, low resistance and strength, costly and also high maintenance cost. Concrete tiles weigh more than clay tiles, though the high density might not seem like a problem at first but the extra weight concrete roof tiles add onto the house can really cause problems with structural durability and over time the house might not be able to even support the weight of the roof anymore.

Common ones in use are: metal, asphalt, wood, ceramic, polymers and quite recently concrete has been explored as a suitable material and found to be useful.

This concrete roof tile used cement as the major classical binder in construction industry is very expensive. This is because of phenomenal population growth and urbanization which have triggered high demand of cement for several construction purposes to meet up with the need to expand infrastructures (Otuoze, et.al 2012).

Besides that, cement is boosting air pollution because have high CO2 emission.

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Therefore the need to connect the gap between demand and high price has warranted the need to investigate the use of cheaper alternative sources.

So, the inclusion of clay in the mix can reduce these used of cement in the concrete mix. It also can cut back the negative impact on the environment and humans contributed by cement used. Besides that, the usage of clay as additive in this concrete roof tile does not need a lot of skilled workers and technological equipment in the process.

One of the most abandoned materials in Malaysia is cellulose non-wood fibrous materials, like rice straw. The National Food Security aims to increase the National Self Sufficiency Level (SSL) of domestic rice production. Malaysia needs to produce around 2.5 million metric tons of paddy annually (Rashid and Shah, 2013). Which means that round the same volume of rice straw was produced in that year (John, 2013). However, the increase in productivity and size of paddy areas, among other things, has led to a huge excess of rice straw where the most efficient manner of disposing of the residue is seen as burning the rice straw in the paddy field. As a result, it is boosting air pollution and serious human health issues due to the emission of carbon monoxide (Allam, et al., 2011). Rather than burning the rice straw, recycling it with a mix of cement forms a sustainable low cost building material, which additionally reduces atmospherically pollution (Allam et al., 2011).

The reuse of abandoned building materials avoids the waste of materials and the environmental problems caused by combustion which is in line with the green environmental protection theme advocated by China (Wang and Yan, 2018).

To avoid such a situation, in this study proposes the utilization of rice straw as a lignocelluloses material to improve and produce concrete roof tile composites as

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method to positively impact indoor conditions of Malaysia and also the resource poor countries of the developing world. Additionally to those advantages, the rice straw might acts as a thermal insulation material for the unpleasant Malaysian weather.

Also, the use of thermal insulation helps to reduce energy costs, while creating pleasant indoor temperatures.

This concrete roof tile composite produce can act as a passive cooling material that can improve indoor thermal quality and also can enhance the mechanical and physical properties such as density, durability, heat absorption, water absorption, strength, and others.

1.4 Research Questions

i. What is the satisfactory of clay and rice straw ratio for concrete roof tile composite?

i. What the physical and mechanical properties of concrete roof tile with clay and rice straw as additional materials?

ii. How the thermal performance of concrete roof tile composite

iii. How to get thermal performance of actual house model data used the simulation by IESVE software.

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This study is designed to develop the performance of concrete roof tiles and allow this material suitable for low-cost housing applications. After identifying the main factors that contribute to the inferior properties of concrete roof tile, this study proposes a material for enhancing concrete roof tile physical, mechanical and also thermal performance.

The proposed method involves the following steps to improve the concrete roof tile mix: The first phase involves enhancing the properties clay before incorporating into the concrete roof tile mix. In this process, the raw clay was filtered the impurities and dirt.

The second phase involves modifying the concrete roof tile mix by the inclusion of fibres. In this study, rice straw fibre was used at various lengths and volume fractions to help modify and improve the properties of concrete roof tile.

The third phase is employs a suitable experimental programme to characterise the behaviour that leads to concrete roof tile composite as well as to fully understand the feasibility and effectiveness of the modification in enhancing concrete roof tile composite in physical, mechanical, and thermal performance.

The objectives of this study are as follows:

ii. To determine the recommended ratio of clay and rice straw in producing a newly concrete roof tile composite,

iii. To examine the physical and mechanical properties of concrete roof tile with clay and rice straw as additional materials,

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iv. To evaluate thermal performance of the concrete roof tile composite in order to reduce heat transfer into the building

v. To examine thermal performance of actual house model and simulate data by using IESVE software.

1.6 Scope and Limitation of the Research

The major scope and limitation of this research work is to produce a concrete roof tile composite, which is able to enhance indoor thermal performance due to low heat absorption and high solar reflection. The concrete roof tile composite was produced from clay that has been cleaned of impurities derived from Sayong, Kuala Kangsar, Perak. This clay was dried under the heat of sun and processed through various crushing stages and then sieved using vibrator sieve to obtain the required particle size. Another material is rice straw that was collected from the paddy fields at Kuala Kurau, Perak. This material is collected, washed with water, dried under a sun drying, cut off and sieved using a vibratory sieve to obtain the required size.

i. The first approach involves improving the properties of concrete roof tile composite by combining two different materials, cement and clay as a binder in a mortar. Unfired clay was used as additional material in a concrete mix with three different percentages at 10%, 20%, and 30% by weight of the total cement content. The effects of these materials on the concrete roof tile composite mechanical and physical properties are determined. Several tests were conducted to investigate these properties, such as a test for particle size

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distribution, absorption, density, impact value, flexural and compressive strength.

ii. The second stage involves modifying the concrete roof tile composite mix by the inclusion of rice straw fibres. In this study, short rice straw fibres were added to the appropriate volume fractions to help modify and improve the properties of concrete roof tile composite in the strength, thermal absorption, and density. The method and mix proportion of concrete roof tile were designed according to the Malaysia Standard 10D036R1 (2014).

Accordingly, fourthly series of concrete mixes were designed and prepared depending on the volume fractions of the fibre content used. Three different lengths of rice straw at 0.1-2.0cm, 2.1-4.0cm and 4.1-6.0cm were tested in three different amounts of percentages at 1%, 1.5%, and 2%, according to the volume fractions concept. Unfired clay was used as additional material in a concrete mix with three different percentages at 10%, 20%, and 30% by weight of the total cement content.

iii. The assessment of the engineering properties of concrete roof tile composite after adding rice straw include determining the slump of fresh concrete mix, physical and mechanical strength of hardened concrete, namely, water absorption, density, drying shrinkage, compressive strength, flexural strength and impact resistance. The proportion of the concrete roof tiles mixture complied with ASTM C1492-03 (2016). It was based on constant effective water/cement ratio of 0.45-0.61 for all concrete roof tile mixtures, to achieve a target flow diameter range of 105-115mm and a compressive strength of

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2,500 psi (17.2 MPa) on the 7 days. The experimental tests examined the mechanical, physical and thermal properties of the cube sample exposed to water and plate sample is curing in 40⁰C of the room conditions were conducted for up to 300 days. The test is to investigate the impact behaviour of the concrete plate was conducted after the entire tested sample reached at the testing age of 28 days. Concrete porosity and microstructure test is not carried out in this study.

iv. The final aspect of the study involved the method used to measure thermal performance properties of four types of concrete roof tile where the first is a normal mix (cement and sand), second is normal mix with clay, third is normal mix with rice straw and lastly normal mix with clay and rice straw.

Thermal properties of this four mix was conducted using Hot Disk Thermal Analyzer and essential values such as thermal conductivity, thermal diffusivity and specific heat capacity were recorded. Besides that, in this stage a model house was used to examine roof thermal performance and the best of concrete roof tile composite was installed as a roof covering.

Thermocouple measurement tools are placed in a model house. The temperature difference between the interior and exterior roof surface was recorded. Besides that, AEMC 1950 Thermal Imaging Camera 80 x 80 with Bluetooth was used to automatically display the cool and the hot spot values at the minimum and maximum cursor position. It displayed point that fell in the same temperature range and the displayed colour blue, red, brown or yellow as defines the range and tolerance. Simulate data from field test data

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